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UltraALLOY TM
STAINLESS STEEL CAPILLARY COLUMNS |
- High temperature
stability
- Highly inert
deactivated inner surface
- Exceptional mechanical
durability-cannot break!
- Perfect for field use
or high vibration situations
- Can be tightly coiled
(3 inches) for portable GCs
- Ideal for use in SRI
Instruments GCs
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The inertness of Ultra
ALLOY TM
stainless steel columns matches
that of fused silica and is derived from a patented,
multi-step manufacturing process which utilizes a
five-layered pretreatment of the inner surface of the
stainless steel.
SEM
images of Ultra-Alloy tubing surface,
before
deactivation (left)
and after deactivation (right).
Each
layer is chemically stable at elevated temperatures
and has equal to, if not superior, mechanical
properties to that of the steel tubing. The layers
are less than 0.01 microns thick and are chemically
bonded together. Stationary phases are then easily
bonded to this stable inert surface resulting in
superbly deactivated columns which compare directly
to fused silica columns.
| UAC-1,
10M. x 0.25mm x 0.25um film |
DB-1,
10M. x 0.25mm x 0.25um film |
| 1st injection |
81st injection |
1st injection |
20th injection |

A comparison of a UAC-1 (methyl
silicone) stainless steel column and a fused
silica DB-1 column.
Consecutive injections of 5% rapeseed oil,
120oC isothermal, split injection. |
Accordingly,
Ultra ALLOY TM capillary
columns offer unsurpassed inertness and mechanical
durability and are suitable replacements for fused
silica capillary columns. Unlike other stainless
steel columns on the market, Ultra- ALLOY TM columns are
not lined with fused silica (see photo below) which
can crack or flake-off when flexed or bent thus
exposing active sites. As a result, the Ultra-ALLOYTM columns can be
tightly coiled to accommodate even the smallest of GC
oven designs.
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|
SEM
Photo of stainless steel tubing
with fused
silica layer.
(Photo courtesy of Valco
Instruments) |
Ultra ALLOY TM columns are
available in the standard 0.25mm and 0.50mm I.D.s
The tables below list the
available bonded phases, films and maximum
temperatures. Go to the Ultra ALLOY TM Ordering
Information Section for available
lengths and pricing. Deactivated
Ultra ALLOY TM tubing is also
available for transfer lines and guard columns.
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AVAILABLE COLUMN CONFIGURATIONS |
| |
|
Film
Thickness (µm) |
Maximum
Temp. oC |
| Phase Code |
Composition |
0.25mm I.D. |
0.50mm I.D. |
Isothermal |
Programmed |
| UAC-1 |
Methyl silicone |
0.15, 0.25, 0.5, 1.0* |
0.15, 0.25, 0.5, 1.5*, 5.0* |
350 / 380 |
330* / 360 |
| UAC-1HT |
Methyl silicone - high
temperature |
0.15, 0.25 |
0.15, 0.25 |
400 / 420 |
|
| UAC-5 |
Methyl 5% phenyl silicone |
0.15, 0.25, 1.0* |
0.15, 1.5* |
350 / 380 |
330* / 360 |
| UAC-DX30 |
Carborane siloxane (Dexsil 300) |
0.15 |
0.15 |
450 |
|
| UAC-17 |
Methyl 50% phenyl silicone |
0.15, 0.25 |
1.0* |
370 / 390 |
350* / 370 |
| UAC-CW |
Polyethylene glycol (Carbowax) |
0.25 |
1.0* |
260 |
240* |
| UAC-TRG |
Triglyceride phase |
0.15 |
|
370 / 380 |
|
| UAC-502 |
Volatile Organics phase |
1.0 |
3.0 |
270 |
|
| UAC-624 |
Volatile Organics Phase |
1.0 |
3.0 |
280 |
|
| UAC-DIDP |
Diisodecyl phthalate
(non-bonded) |
0.4 |
|
150 |
|
Click here for Ultra-ALLOY ordering information
Ultra
ALLOY and UA are trademarks of Frontier Laboratories,
Fukushima, Japan.
Send mail to Webmaster@quadrexcorp.com with questions or comments
about this web site.
Copyright © 1999 Quadrex Corporation
Web Site Designed By Bob White From Duet Productions Ltd.
(We are not
affiliated in any way with the Quadrex Corporation (Symbol: QUAD)
that appears on the stock market.)
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