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The
SRI Method TO-14 air concentrator is identical to the Method
5030 style Purge & Trap, but without the liquid purge
vessel. The
purge vessel is replaced with a vacuum pump interface
so an external vacuum pump may be attached to the downstream
side of the traps to automatically load a gas sample under
control of the PeakSimple data system.
Gas
samples may be contained in tedlar bags, canisters or may be
sampled directly from the source.
The
vacuum pump is operated for several minutes or more to pass
100-200 ml/minute of gas through the traps where the organics
are retained. Several liters or more may be concentrated
depending on the ultimate detection limit required.
An
optional off-line tube desorber may be added to the
concentrator for applications where the sample is already
trapped off-line on charcoal, Tenax or molesieve sampling
tubes. The off-line tube is connected to a heater block and
purge gas fittings mounted on the top of the concentrator.
Under control of the PeakSimple data system ( for
reproducibility ) the tube is heated and its contents flushed
into the traps of the concentrator.
This process can take several minutes depending on the
trapping material in the tube.
The re-trapped organic analytes are then efficiently
desorbed onto the GC column for separation and quantitation.
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