HIGH
PURITY
GAS GENERATOR SYSTEMS
FREQUENTLY
ASKED QUESTIONS
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General
Information
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How
do the Generators work?
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The
Hydrogen Generator works on the principle of
disassociation of water through an ION Exchange
Membrane to produce ultra-high purity gas. All
other Generators use a combination of molecular sieves
and filtration to produce different gases suited to
your instruments.
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Are
the Generators noisy?
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The
Hydrogen Generators are completely silent.
Nitrogen or Zero-Air Generators using house air
supplies are also completely silent. Generators
utilizing the built-in air compressors (part numbers
noted with an ''A" suffix) are exceptionally
quiet and feature a quiet purge (where necessary).
Any noise comes from the cycling of the
on-board air compressors, where applicable.
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What
is the life expectancy of a Generator?
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All
Generators have a life expectancy of 7-10 years.
Keeping in mind that the ION Exchange Membranes from
Hydrogen Generators currently in use have been running
continuously for 12 years. The sieves used in
the other Generators can be regenerated and will last
indefinitely, providing the compressed air supply is
always clean and dry.
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Is
there any required maintenance?
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All
Generators feature minimal maintenance requirements
such as the periodic changing of filters.
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How
safe are the Generators?
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All
Generators are built with lab safety in mind, and have
safety features applicable to each gas. All Gas
Generators are controlled by a mass flow controller,
so it is not possible to overload the system at any
time or produce low quality gases below
specifications.
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Can
outlet pressures be adjusted?
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Yes,
on all Generators, either by using the Pressure
Regulator provided or by using an additional Line
Regulator at the instrument.
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What
technical Support do you provide?
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Quadrex
Corporation or Peak Scientific’s Technical
Information Support Staff are always available to help
you with your questions and problems. Please see
our Contact page if
you have a technical inquiry
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What
about installation procedures?
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Installation
for each Generator is easy and only requires a
connection to an electrical outlet, and dependent upon
the Generator, either to your compressed air supply or
to a supply of water.
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Does
air need to be pre-filtered before entering the
Generator?
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Yes,
in all cases, the Generators are supplied with
Pre-filters. However, we recommend that, if your
house compressed air supply is extremely oily and
dirty, that a further Pre-filter be put in the line to
ensure absolute air quality.
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Can
I hook up a back-up cylinder?
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Yes,
this allows the system to be totally redundant in the
event of a power failure or breakdown. It is
suggested that the cylinder be hooked up using an
Automatic Changeover Switch, so that it will kick in
in the event of a loss of pressure at the Generator.
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What
happens if purity drops below a certain level?
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Your
first indication will be that you will notice a change
in results produced at your instrument. The
Generators should be checked, filters changed, sieves
and membranes examined and changed if necessary.
The Generators can be supplied with optional Oxygen
Analyzers, if necessary.
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Why
should I buy from Peak Scientific?
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Peak
is dedicated only to Gas Generators. Years of
experience and knowledge give Peak the ability to
satisfy your technical, commercial and personal
requirements.
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Hydrogen
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How
safe are the Generators?
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The
Generators are designed with your safety in mind.
They feature automatic shut-down and visual/audible
alarms to indicate high pressure or gas leaks both
inside and outside the instrument.
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How
is the oxygen separated from hydrogen in the
Generator?
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The
Generator features an ION Exchange Membrane in which
hydrogen is produced. Oxygen is separated from
hydrogen and is bubbled off with water into a holding
chamber before it is automatically vented at the rear
of the instrument.
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Do I need to use caustic solutions?
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No,
the Peak Hydrogen Generator runs on deionized water.
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How
much gas is stored in the Generator during operation?
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Maximum
quantity of gas that can be stored in the Generator at
any one time cannot exceed 400 ml at a maximum
pressure of 100psi.
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What
is the purity level?
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Purity
of gas is >99.9999% at maximum flow.
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Does
it make any noise?
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No,
the Generator is completely silent.
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How
low a grade of water can I use?
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The
Generator will accept deionized water @ <1µS/cm
and will produce >99.9999% purity gas. DO
NOT USE TAP WATER, tap water will damage the Cell.
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How
do I load the Generator with water?
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The
Generator features an automatic loading pump which,
when attached to an external water supply, will pump
water into the Generator, as required, allowing the
user less maintenance. If the water supply runs
low, an audible alarm will sound in the Generator to
alert the user.
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Can
I load water manually?
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Yes,
simply hook up your water supply to the back of the
instrument and the internal pump will fill the chamber
inside the Generator, providing up to 350 liters of
hydrogen from a single charge.
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What
are my options for hooking up to an external water
source?
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The
Generator can be hooked up to a lab deionized water
supply @ <1µS/cm or an external tank of water,
which, if necessary, can be situated below the height
of the Generator.
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How
often does the reservoir need to be filled?
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A
single charge of water in the Generator will supply up
to 350 liters of hydrogen. This will depend on
your usage of gas.
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What
happens in the event of a power failure?
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The
Generator will automatically stop production of gas
and shut down. When power is restored, the
Generator will go into standby mode and sound an
audible alarm, but will not start producing gas until
an attendant manually switches the instrument back on.
However, in cases where gas is being used for a
carrier and where a continuous flow is vitally
important, the Generator features a microprocessor
control that allows the user to manually reset the
system so that in the event of a power failure, the
Generator will automatically restart.
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How
often does the desiccant need to be changed?
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Desiccant
will turn from orange to green indicating that a
change is necessary. This can take anywhere from
1 week to 6 weeks, depending on the size of the
Generator and the gas consumed.
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Can
I regenerate the desiccant?
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Yes,
up to three times, at which point we would recommend
the addition of a new desiccant to the drying
cartridge.
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What
is the Maintenance Schedule?
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Maintenance
is limited to a change of the desiccant cartridge, as
required. This can be anywhere from weekly to
bi-monthly, depending upon the volume of gas consumed.
For example, the HG200, running continuously for 24
hours per day, will only require a desiccant change
once per month.
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What
technical support do you provide?
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Quadrex
Corporation or Peak Scientific’s Technical
Information and Support Staff are always available to
help with your questions and problems.
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What
is the warranty?
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A
full 12 month warranty.
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What
about installation?
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Installation
is easy – simply connect the Generator to your
electrical supply and an external water source. The
Generator will automatically pump water into the
holding chamber, then, after a 4 minute “System
Check”, the Generator will automatically begin
producing ultra-high purity gas. Pressure can be
regulated at the rear of the instrument.
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Why
should I buy from Peak Scientific?
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The
Peak Hydrogen Generators are the only Generators
available with flows ranging from 200-600 cc/min.
The ION Exchange does not require any caustic
solution. Display indicates gas production and
indicates leaks in the system or line. Safety
devices indicate over-pressure and leaks.
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Nitrogen
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What
is the purity level of gas?
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Purity
level is >99.999% purity at maximum flow, which is
equivalent or better than N2 supplied by
industrial gas companies in cylinders. The
nitrogen has an O2 level <10 ppm and a
moisture level <1ppm.
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How
does the Generator work?
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The
Generator uses pressure swing adsorption technology
and a proprietary carbon molecular sieve.
Compressed air is fed into the sieve bed and passes
through the column, where all impurities are removed.
Pure nitrogen exists at the top of the column and is
stored in a small reservoir. At a specified
time, a small amount of ultra-high pure nitrogen is
used to back flush the sieve bed and regenerate the
system. Gas flow is continuous and controlled by
a mass flow controller.
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What
if I don’t need 99.999% purity?
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All
of the Generators can be adjusted to meet your purity
and flow requirements at the factory before shipment.
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What
happens if I turn it off and there is power failure?
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If
you happen to turn off the Generator, you can simply
turn it back on and start producing ultra-high purity
gas immediately. In the event of a power failure
for an extended period, it is recommended that the 4
hour purge be repeated to ensure absolute gas quality.
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Does
it make any noise?
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The
Generators are available with or without an integral
air compressor. Therefore, using your own house
air supply means that the Generator will be totally
silent, except for a “quiet purge” once every 2
minutes. If the Generator features an integral
air compressor, it also runs exceptionally quietly,
with a noise level of 59d(B).
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Can
I fill an external reservoir with gas?
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Yes,
you can. Depending on your flow requirements for
various instruments, this can sometimes be a good way
of achieving a continuous flow of gas at varying
pressures.
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Do
I ever need to change the sieve?
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No,
the Sieve is completely sealed in the nitrogen tubes
and is only affected by exposure to oil, sunlight or
the atmosphere. If you are considering using
your own compressed air supply to run the Generator,
we strongly recommend the use of oil-free air or
pre-filters to remove all oil from the system before
entering the Sieve Beds.
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Is
it easy to install?
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Yes,
simply hook up the Generator to an electrical supply,
switch on and allow for a 4 hour purge to achieve
99.999% purity before hooking the Generator up to your
instrument, using the 1/8” connections at the side
of the Generator.
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What
is the warranty?
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A
full 12 month warranty.
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If
I am using lab air, what are the requirements?
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If
you are using your own compressed air supply, a
continuous pressure of 100 psi is required with
filtration down to .01 micron before entering the
Generator. In order to size your compressor
requirements correctly; please contact us.
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Why
should I buy from Peak Scientific?
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Peak
Scientific Instruments Ltd is dedicated only to Gas
Generators. Years of experience and knowledge
give Peak the ability to satisfy your technical,
commercial and personal requirements.
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How
do you guarantee purity?
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Purity
is guaranteed with a mass flow controller, with which
you cannot overflow the system, thereby ensuring
constant purity.
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Zero Air
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How
are methane hydrocarbons removed?
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Methane
hydrocarbons are removed by catalytic oxidation using a platinum
catalyst and heater module to convert total hydrocarbons to CO2
and water.
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How
easy is it to use?
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Generators
are easy to install and use. Simply attach to an electrical supply
and hook up your inlet and outlet air lines. Turn the Generator on
for 20 minutes to warm up the “oven” and then start using the
Generator to produce zero air with THC <.1 ppm.
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Does
it make any noise?
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No,
if you are using a house air source, the Generator is completely silent.
Otherwise there is minimal noise from the cycling of the integral
air compressor.
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What
compressed air supply do I need?
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Anywhere
from 10-150psi.
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How
long is the warm-up period?
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Twenty
minutes, after which time the Generator will provide a continuous flow
24 hours per day.
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What
is the warranty?
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A
full one year warranty on parts and labor is included.
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Is
this system serviceable?
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Peak
Heater Rod and Thermocouple are removable.
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What
technical support do you provide?
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Quadrex
Corporation or Peak Scientific’s technical information and support
staff are always available to help you with your questions and problems.
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What
is the difference between zero air and pure air?
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Zero
air is air with a total hydrocarbon content of <.1ppm (as CH4).
Pure air is dry and clean with a hydrocarbon content of <3ppm, but
methane levels may be as high as 10 ppm.
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Does
the Generator cabinet get extremely hot during operation?
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No,
the box will be warm to touch but does not create any hazard or excess
heat.
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Where
do hydrocarbons go?
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Hydrocarbons
are converted to water and CO2 by the catalytic oxidation.
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What
is the minimum air flow requirement to power the Generator?
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Dependent
on your requirements for zero air, as low as 10 psi.
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Copyright © 2002 Quadrex Corporation
Web Site Designed By Bob White From Duet Productions Ltd.
" We
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market. "
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